High precision Resistivity Measurement of thin epitaxial layers and substrates

Aim

Measuring the resistivity of epitaxial layers on highly doped semiconductors is a huge challenge, but crucial for several reasons:

  • Material quality assessment, as an insight in the structural and electronic quality

  • Doping density verification

  • Device performance prediction

  • Extraction of material parameters as carrier concentration

  • Process development and simulation of doping models

  • Detection of contaminations, process drift and inhomogeneities and defects

Hence the availability of such a measurement with precision and reproducibility is critical for advanced semiconductor applications. So far only destructive methods with no or low spatial resolution as Mercury CV are available.

Solution

Together with Toptica, Fraunhofer ITWM and Fraunhofer IISB and the TU Bergakademie Freiberg a mapping tool based on THz Time-Domain spectroscopy (TDS) in a reflection geometry was developed which enables high-precision mappings with a resolution of 1 mm for all kinds of epitaxial layers on highly doped materials (Si, SiC and more). 

This new THz method enables the measurement of the resistivity for bulk wafers in a range of 0.1 to 100 Ωcm or for epitaxial layers with a thickness of > 10 µm and a doping density of 8 x 1015 cm-3 to 4 x 1018 cm-3. Even the simultaneous measurement of substrate and epitaxial layer is possible. The measurement is contactless and destruction free and therefore ideal for industrial applications [1].

Application example

Figure 1 shows an exemplary mapping of the doping density of an 4 inch, highly doped 4H-SiC substrate with a 11 µm thick epitaxial layer. The growth facet in the substrate can be clearly detected as well as the radial gradient in the doping of the epitaxial layer. The edge exclusion is appr. 3 mm and a reproducibility of better than 99 % is reached.

A comparison with mercury CV measurements shows a very good agreement (Figure 2). The deviation is within 0.56 %.

THZmap

Supported by

Our Partners


Related Materials: Si, SiC, and more

Related Solutions and Industries: Epitaxial Layers & Thin Films

Get in touch

Do not hesitate to contact us – we are available to assist you with any inquiries or requests.

Use our inquiry tool or reach out via email:
sales@freiberginstruments.com